A total workflow for multi-class, multi-residue analysis of pesticides in fatty food matrices

Join this webinar to learn strategies for sample preparation, instrument method development and optimization, plus workflow applicability to their practical applications

16 Jul 2020
Diane Li
Assistant Editor

Expert insights

The development of multiresidue methods for the determination of fat‑soluble pesticides in edible oil at low levels is still a challenging issue. Much effort has been invested in extraction of hydrophobic pesticides from sample matrices and cleanup of lipids prior to analysis. Matrix co-extractives deposit on the instrument flowpath, decreasing analyte sensitivity by degrading the flowpath inertness. An efficient cleanup of the oil extract is necessary to improve column lifetime and reduce instrument maintenance frequency.

In this upcoming webinar, Limian Zhao and Dr. Xia Yang from Agilent Technologies will present a complete workflow for the analysis of multi-class, multi-residue pesticides in fatty food matrices including milk, salmon and vegetable oils. From sample preparation through to analysis using either GC-MS/MS, LC-MS/MS or both, the entire workflow is designed to provide a simple and efficient sample extraction and fatty food matrix cleanup with accurate and precise analysis for both LC and GC amenable pesticides.

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In this webinar, you will:

  • Understand the challenges posed by fatty food matrices and strategies for both sample preparation and analysis
  • Learn sample preparation methodologies for efficient extraction of pesticides from fatty foods
  • Learn about common Agilent GC-MS/MS and LC-MS/MS system performance for analysis of pesticides
  • A total workflow for analysis of pesticides in fatty food matrices that can be used directly for practical applications

Who should attend

  • Scientists in food labs responsible for method development and sample analysis
  • Lab managers in food labs
  • Bench chemists regularly carrying out sample preparation

The live webinar takes place on Tuesday, July 28, 2020, at:

14:00 BST
09:00 EDT
06:00 PDT
15:00 CEST

Scheduling conflict? No matter, register to receive an on-demand link to watch later>>

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Gas ChromatographyGas chromatography (GC) is an analytical technique used to separate and quantitate mixtures of small and volatile compounds. Gas chromatographs or GC systems include components such as GC columns, detectors, pumps and autosamplers. Choose from packed or capillary GC columns, flame ionization (FID), photoionization (PID) electron capture detectors and selective or non-selective detectors. Find the best gas chromatographs in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.UHPLC and HPLCHigh performance liquid chromatography (HPLC) and ultra high performance liquid chromatography (UHPLC), also known as UPLC, are analytical techniques used to separate, identify and quantitate components of complex mixtures including biological samples such as proteins and lipids as well as chemical mixtures of pesticides, drugs and oils. Both techniques are liquid chromatographic methods but differ by operating pressures (HPLC < 6000 psi < UHPLC ). Components of HPLC and UHPLC systems include columns, detectors, pumps, autosamplers and column heaters. Explore a range of UHPLC and HPLC columns for your specific sample needs including reverse phase, normal phase, ion exchange, HILIC, ion exclusion and size exclusion columns. For more specialized HPLC, explore FPLC, countercurrent LC and simulated moving bed systems. Find the best UHPLC and HPLC equipment in our peer reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.LC-MSLC-MS (liquid chromatography-mass spectrometry) systems and equipment are used for separation and quantitative analysis of complex mixtures, combining liquid chromatography and mass spectrometry. Quantify proteins, contaminants, pesticides or screen for drug metabolites with a high level of sensitivity. LC-MS systems and equipment include reverse phase, normal phase and specialized columns integrated with various MS detectors such as time-of-flight (TOF), quadrupole, orbitrap or ion trap mass analyzers. LC-MS/MS instruments equipped with a qTOF or triple quadrupole analyzer give greater sensitivity and resolving power to your analysis. Find the best LC-MS equipment in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Food and Beverage AnalyzersFood and Beverage Analyzers are commonly used to provide information about the chemical composition, structure and physical properties of food materials.Food and Beverage ProcessingFood and Beverage Processing involves the preparation of food products for further analysis. Typical instrumentation includes blanchers, color sorters, cookers, grinders, and refrigeration. These are used to replicate the processes commonly used in the commercial preparation of food and beverages.Particle CharacterizationParticle characterization instruments are used to determine particle size distribution, shape, surface area, zeta potential, density and porosity of particles and materials. Multiple tecchniques are available for determining particle size, shape and count including dynamic light scattering (DLS), laser diffraction, electrozone (Coulter technique), imaging particle analysis and single particle optical sensing. Determine the density of your material with a gas pycnometer or examine its surface area and porosity with gas adsorption analyzers and mercury porosimeters. Find the best particle characterization instruments in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.GC-MS GC-MS (gas chromatography-mass spectrometry) instruments and equipment are used to separate, quantify and identify mixtures of small and volatile compounds, such as polycyclic aromatics, fatty acids and alcohols. Often used in drug detection, forensic investigation and environmental analysis for pesticides and contaminants, GC-MS is a powerful addition to your lab’s analytical capabilities. GC-MS/MS instruments equipped with a qTOF or triple quadrupole analyzers can give greater sensitivity and resolution to your analysis. Find the best GC-MS instruments and equipment in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.PesticidesPesticides are used to protect crops from diseases, pests and unwanted plants. They are classed as persistent organic pollutants (POPs) and can be harmful to humans. The Environmental Protection Agency (EPA) currently regulates the use of pesticides in the USA. Food TestingFood testing refers to a variety experiments including PCR, mass spectrometry, processing, QuEChERS, analyzing and Kjeldahl.Food QualityFood quality refers to the attributes of food that influence its safety, nutrition, and taste. Monitoring and ensuring food quality are essential in production to meet health regulations and consumer expectations. Techniques like spectroscopy, chromatography, and microbial testing are used to assess food properties and detect contaminants. Browse our peer-reviewed product directory to find food quality testing solutions; compare products, check reviews, and get pricing directly from manufacturers.Chemical Residues in FoodGC-MSGas Chromatography-Mass Spectrometry (GC-MS) combines the separation power of gas chromatography with the detection capabilities of mass spectrometry, allowing for the analysis of complex mixtures. It is widely used in environmental, forensic, and pharmaceutical analysis. Explore GC-MS systems in our peer-reviewed product directory; compare products, check reviews, and get pricing directly from manufacturers.
A total workflow for multi-class, multi-residue analysis of pesticides in fatty food matrices