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Trace Determination of Organo-Phosphorous Pesticides in Olive Oil by GC Analysis through PTV Backflush / FPD

Trace Determination of Organo-Phosphorous Pesticides in Olive Oil by GC Analysis through PTV Backflush / FPD

20 Sept 2015

This paper describes an alternative way to effectively and rapidly analyze Organo-Phosphorous Pesticides (OPPs) in oils eliminating any interference with the heavy fraction. OPPs are widely used in agriculture, due to their relatively low cost, broad spectrum of activity, and high impact on insects compared to other pesticides. However, because the OPPs are well known to cause irreversible effects on the nervous system (reduced activity of neurotransmitters), their possible presence as trace residues in food must be strictly monitored.

Thermo Scientific™ TRACE™ 1300 Series GC System

Thermo Fisher Scientific

The Thermo Scientific TRACE 1300 Series GC offers the most versatile gas chromatograph platform in the market, with unique "instant connect" modularity for ground-breaking ease of use and performance, setting a new era in GC technology.The Thermo Scientific TRACE 1300 Series GC is the ideal budget-conscious investment for the basic routine laboratory when lower operator expertise requires ease of use with minimal instrument interaction. Its simplified user-interface is also ideal for 24/7 operations that require single-button start/stop/maintenance local interactions while maintaining full programmability through the networked control software.Interchangeable modules free your laboratory from the challenges and constraints of the past. Remove the complexity and eliminate the need for specialized service assistance or new system requirements with modular injectors and detectors.Thermo Scientific Trace 1300 Series GC Features: Analyze dirtier matrices with minimum cleanup using the system's robust injector technology Analyze trace concentrations with smaller injection amounts and minimum preconcentration results using enhanced detector sensitivity and micro-volume technology Protect system components and reduce run time and maintenance using optional backflush capabilities Shorten sample cycle times using low thermal mass injectors and detectors and fast oven technology Automate your entire workflow—from pipetting to injection—using a full range of sample handling options Streamline and speed up data analysis using Thermo Scientific™ Dionex™ Chromeleon™ Chromatography Data System (CDS) software Expands easily from single-channel to multi-injector/detector GC configurations Reduces training and startup time with simplified installation, plug-in components, minimal local control and intuitive Chromeleon software Minimizes downtime with easy-access, tool-free modules Reduces operational costs by allowing use of standard consumables Saves energy with low thermal mass and quick start-up Minimizes sample and solvent consumption with micro-volume sample capability Modular design lets you easily reconfigure to meet changing requirements

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Gas ChromatographyGas chromatography (GC) is an analytical technique used to separate and quantitate mixtures of small and volatile compounds. Gas chromatographs or GC systems include components such as GC columns, detectors, pumps and autosamplers. Choose from packed or capillary GC columns, flame ionization (FID), photoionization (PID) electron capture detectors and selective or non-selective detectors. Find the best gas chromatographs in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Mass SpectrometryMass spectrometry (MS) is a powerful analytical technique used to identify and quantify molecules based on the mass-to-charge ratio of gas-phase ions. It provides detailed information about the structure, composition, and properties of compounds and is widely used across fields such as environmental monitoring, materials science, drug discovery and development, food and beverage testing, and wider chemical research. Key MS techniques include tandem mass spectrometry (MS/MS), liquid chromatography–mass spectrometry (LS-MS) and inductively coupled plasma (ICP-MS). Choosing from these wide range of techniques and technologies can be a daunting task, so keep up to date with scientific applications, performance expectations, and customer reviews here all in one place. Visit our product directory to receive quotes direct from the manufacturer. Environmental Monitoring and TestingEnvironmental monitoring and testing uses handheld portable analyzers, kits, spectrometers or chromatography systems for air, water, soil, food and other sample testing. Useful features of analyzers such as BOD and COD include portability, easy calibration, automation and sensitivity.  Environmental test kits for pH, water, moisture, etc, should be accurate, sensitive, reliable, fast and easy to use.Solid-Phase ExtractionSolid-phase extraction (SPE) is used for clean-up, extraction and concentration of semi-volatile or non-volatile analytes from complex mixtures including blood, urine and food samples. Multiple formats are available for conducting SPE, including prepacked SPE cartridges, disks and microplates, as well as SPE sorbent powders for manual packing. SPE systems can be used to automate the process and extract multiple samples at once. Solid-phase microextraction (SPME) and supported liquid extraction (SLE) products are also available in the same formats. Find the best SPE, SLE and SPME equipment in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Food and Beverage AnalyzersFood and Beverage Analyzers are commonly used to provide information about the chemical composition, structure and physical properties of food materials.Food and Beverage ProcessingFood and Beverage Processing involves the preparation of food products for further analysis. Typical instrumentation includes blanchers, color sorters, cookers, grinders, and refrigeration. These are used to replicate the processes commonly used in the commercial preparation of food and beverages.GC-MS GC-MS (gas chromatography-mass spectrometry) instruments and equipment are used to separate, quantify and identify mixtures of small and volatile compounds, such as polycyclic aromatics, fatty acids and alcohols. Often used in drug detection, forensic investigation and environmental analysis for pesticides and contaminants, GC-MS is a powerful addition to your lab’s analytical capabilities. GC-MS/MS instruments equipped with a qTOF or triple quadrupole analyzers can give greater sensitivity and resolution to your analysis. Find the best GC-MS instruments and equipment in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.PesticidesPesticides are used to protect crops from diseases, pests and unwanted plants. They are classed as persistent organic pollutants (POPs) and can be harmful to humans. The Environmental Protection Agency (EPA) currently regulates the use of pesticides in the USA. AgricultureAgriculture research focuses on improving food production, crop management, and sustainability. This includes plant breeding, pest control, and soil health studies. Explore agriculture research tools in our peer-reviewed product directory; compare products, check reviews, and get pricing directly from manufacturers.Food ContaminationFood contamination refers to the presence of harmful substances or pathogens in food, posing risks to human health. Contaminants can be biological, chemical, or physical, and their detection is crucial for ensuring food safety. Advanced testing methods like PCR, chromatography, and spectroscopy are used to identify contaminants in food products. Browse our peer-reviewed product directory to find the best solutions for food contamination detection, compare products, check reviews, and get pricing directly from manufacturers.Olive OilOrganic CompoundsOrganic compounds are carbon-based molecules that form the building blocks of life. These include hydrocarbons, lipids, proteins, and nucleic acids. Understanding organic compounds is crucial in chemistry, biochemistry, and pharmacology. Explore organic compound analysis tools in our peer-reviewed product directory; compare products, check reviews, and get pricing directly from manufacturers.