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A Fast Sample Preparation Workflow for Veterinary Drugs Analysis in Salmon

Agilent Technologies
21 Jul 2019

In this application note, Agilent outlines a simple, fast, and robust sample preparation workflow and analytical method that was developed for the analysis of seven classes of 53 widely-used veterinary drugs in salmon. A one-step solvent extraction followed by pass-through cleanup with Agilent Captiva EMR—Lipid was used for the analysis.

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Captiva Filter Cartridges

Agilent Technologies

Filtration is simple, versatile, and necessary to prevent clogging of HPLC columns. Captiva's unique dual depth filtration media provides complete removal of precipitated proteins and outstanding resistance to sample clogging.

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Captiva 96-well Collection Plates and Cover

Agilent Technologies

Captiva 96-well Collection Plates are specially designed for use with Captiva Filtration Plates, SPEC SPE 96-well Plates and Bond Elut 96-well Plates. The 1 mL capacity provides the volume needed to collect all of your filtrate or eluate. Captiva Pierceable 96-well Silicone Covers are easily applied to completely seal the plates. This ensures no sample loss due to spillage or evaporation, and no sample contamination. The silicone is specially designed for 96-well auto injectors, providing easy piercing and removal.

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Sample PreparationSample preparation can improve the quality and speed of separation techniques. Products to assist sample preparation include filtration equipment, evaporators, membranes and sieves.LC-MSLC-MS (liquid chromatography-mass spectrometry) systems and equipment are used for separation and quantitative analysis of complex mixtures, combining liquid chromatography and mass spectrometry. Quantify proteins, contaminants, pesticides or screen for drug metabolites with a high level of sensitivity. LC-MS systems and equipment include reverse phase, normal phase and specialized columns integrated with various MS detectors such as time-of-flight (TOF), quadrupole, orbitrap or ion trap mass analyzers. LC-MS/MS instruments equipped with a qTOF or triple quadrupole analyzer give greater sensitivity and resolving power to your analysis. Find the best LC-MS equipment in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Food and Beverage AnalyzersFood and Beverage Analyzers are commonly used to provide information about the chemical composition, structure and physical properties of food materials.Veterinary DrugsFood TestingFood testing refers to a variety experiments including PCR, mass spectrometry, processing, QuEChERS, analyzing and Kjeldahl.Seafood

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A Fast Sample Preparation Workflow for Veterinary Drugs Analysis in Salmon