FERA Takes Analysis from the Laboratory to the Benchtop

SelectScience® spoke to Dr James Donarski, The Food and Environment Research Agency (FERA), at RAFA

30 Jun 2016
Lois Manton-O'Byrne, PhD
Executive Editor

Editorial article

SelectScience® spoke to Dr James Donarski, The Food and Environment Research Agency (FERA), at RAFA

With food safety testing and routine analysis increasingly carried out by manufacturers themselves, it is very important that you can have the same confidence in the data – and that’s where FERA come in. SelectScience spoke to Dr James Donarski, the Head of Food Authenticity at FERA, about how his research is enabling this transition.

At FERA, Dr Donarski explained, “we use different technologies, from high resolution mass spectrometry to high field NMR spectroscopy, which are incredibly powerful but are also very large”, with some instruments coming in at over 8 feet tall. “They require dedicated staff and liquid nitrogen and helium, and aren’t something you could use in a commercial environment.” However, NMR is an important tool in food testing and confirming authenticity due to the minimal sample preparation, calibration and measurement time required.

Bringing power to the benchtop

“It's important to have a small instrument so you can do your testing on site”, revealed Dr Donarski, and the instrument FERA is using in their method transfer research is the picoSpin™ 80 NMR Spectrometer from Thermo Fisher Scientific. “We can see this being used as an instrument for confirming product specification” Dr Donarski explained, ideal for “routine analysis to be conducted by a non-expert user”.

Discover more news and innovations from RAFA 2015 by visiting our video homepage. Plus, find out more about food safety and authentication testing on our community page.

Have you used the picoSpin™ 80? Share your experience with our worldwide community and write a product review today!

picoSpin™ 80 NMR Spectrometer

Thermo Fisher Scientific

The Thermo Scientific™ picoSpin™ 80 spectrometer provides the power of Nuclear Magnetic Resonance (NMR) spectroscopy in a compact and affordable instrument. The picoSpin 80 spectrometer is simple to operate. It is easy for students and technicians with limited NMR experience to use the power of NMR spectroscopy to identify chemical compounds or elucidate their structure. The instrument’s fluid capillary system is contained within a replaceable cartridge and only requires 40 microliters of a liquid sample. Its temperature-controlled permanent magnet does not require cryogens, eliminating the need for consumables or custom laboratory facilities.picoSpin™ 80 NMR Spectrometer Features: Practical performance – small molecule sensitivity designed for everyday use Personal convenience – portable NMR without waiting for core facility schedules Low cost operation – no cryogens, no deuterated solvents, mains energy supply Unique technology – capillary cartridge system ideal for monitoring chemistry

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NMR and EPR SpectroscopyNuclear magnetic resonance (NMR) spectroscopy is used to resolve the local chemical environment of atomic nuclei with spin, revealing information on molecular structure, dynamic processes and chemical reactions of organic molecules, from proteins to synthetics. Electron paramagnetic resonance (EPR) also known as electron spin resonance (ESR) spectroscopy is used to detect and quantify paramagnetic species in a sample, including free radicals as transition metal ions. By immersing the sample in a strong magnetic field, both NMR and EPR spectrometers probe the sample with either radio waves or microwaves respectively. A range of benchtop, solid-state and time domain NMR spectrometers & EPR spectrometers are available, as well as NMR tubes, NMR solvents, software, coils, and magnets. Find the best NMR & EPR equipment in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Food and Beverage AnalyzersFood and Beverage Analyzers are commonly used to provide information about the chemical composition, structure and physical properties of food materials.Food and Beverage ProcessingFood and Beverage Processing involves the preparation of food products for further analysis. Typical instrumentation includes blanchers, color sorters, cookers, grinders, and refrigeration. These are used to replicate the processes commonly used in the commercial preparation of food and beverages.Routine QuantitationFood SafetyFood safety describes the prevention of food-borne illnesses. Contamination with a variety of pathogens can be prevented with adequate temperature control, hygiene and labeling. Food samples can be tested using GC/MS, HPLC, SPE, and qPCR to ensure their adherence to regulations.Food AuthenticationFood authentication ensures that food products are accurately labeled and free from adulteration or misrepresentation. This is important for consumer safety, quality control, and regulatory compliance. Explore food authentication tools in our peer-reviewed product directory; compare products, check reviews, and get pricing directly from manufacturers.Method Transfer