ResourceSeparations

Prepare Olive Oil Samples for Pesticide Residue Analysis in Half the Time with a Fraction of the Solvent Using dSPE

27 Apr 2017

Olive oil is considered a healthy fat source and is a staple in many recommended diets. However, concerns about potentially negative health effects associated with pesticide residues have increased consumer interest in testing. There are several existing methods for measuring pesticide residues in olive oil, all of which involve sample extraction and cleanup. The common goal of these methods is to remove lipids that are harmful to the analytical system. Efficient sample cleanup procedures are critical to maximizing sample throughput and minimizing labor and material costs. This application note demonstrates the efficiency of a dSPE cleanup procedure, as well as the capabilities of a method-specific analytical column.

Resprep® Resin SPE Disk

Restek Corp.

• 47 mm glass fiber disks embedded with styrene/DVB resin. • For chlorinated, benzidine-containing, or nitrogen-containing pesticides. • Meet requirements of EPA Methods 515.2 and 553.

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Gas ChromatographyGas chromatography (GC) is an analytical technique used to separate and quantitate mixtures of small and volatile compounds. Gas chromatographs or GC systems include components such as GC columns, detectors, pumps and autosamplers. Choose from packed or capillary GC columns, flame ionization (FID), photoionization (PID) electron capture detectors and selective or non-selective detectors. Find the best gas chromatographs in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Sample PreparationSample preparation can improve the quality and speed of separation techniques. Products to assist sample preparation include filtration equipment, evaporators, membranes and sieves.Solid-Phase ExtractionSolid-phase extraction (SPE) is used for clean-up, extraction and concentration of semi-volatile or non-volatile analytes from complex mixtures including blood, urine and food samples. Multiple formats are available for conducting SPE, including prepacked SPE cartridges, disks and microplates, as well as SPE sorbent powders for manual packing. SPE systems can be used to automate the process and extract multiple samples at once. Solid-phase microextraction (SPME) and supported liquid extraction (SLE) products are also available in the same formats. Find the best SPE, SLE and SPME equipment in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.PesticidesPesticides are used to protect crops from diseases, pests and unwanted plants. They are classed as persistent organic pollutants (POPs) and can be harmful to humans. The Environmental Protection Agency (EPA) currently regulates the use of pesticides in the USA. Olive Oil
Prepare Olive Oil Samples for Pesticide Residue Analysis in Half the Time with a Fraction of the Solvent Using dSPE