ResourceSpectroscopy

Investigating cocoa butter crystallization using rheology and Raman spectroscopy

12 Dec 2023

In this application note from Thermo Fisher Scientific, explore how simultaneous rheology and Raman spectroscopy (RheoRaman) measurements were used to examine the isothermal crystallization of cocoa butter. The results indicate that cocoa butter crystallized by first hardening into an amorphous solid. Without coupling these two separate analytical techniques, the observed amorphous–solid to crystalline–solid transformation would have been left undetected.

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Raman SpectroscopyRaman spectroscopy is used to discern the vibrational and rotational states of molecules and hence the chemical composition of a sample by measuring the inelastic scattering of monochromatic light. Explore a range of Raman spectrometers, including handheld/portable Raman spectrometers for QC/QA labs and in situ spectrometers for processes. Conduct Raman imaging for microanalysis of mixed samples using a Raman microscope. Raman spectrographs are also available. Find the best Raman spectroscopy products in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Particle CharacterizationParticle characterization instruments are used to determine particle size distribution, shape, surface area, zeta potential, density and porosity of particles and materials. Multiple tecchniques are available for determining particle size, shape and count including dynamic light scattering (DLS), laser diffraction, electrozone (Coulter technique), imaging particle analysis and single particle optical sensing. Determine the density of your material with a gas pycnometer or examine its surface area and porosity with gas adsorption analyzers and mercury porosimeters. Find the best particle characterization instruments in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Rheology
Investigating cocoa butter crystallization using rheology and Raman spectroscopy