ResourceSeparations

In-Tube Extraction Dynamic Headspace (ITEX-DHS) sampling technique coupled to GC-MS for sensitive determination of odorants in water

15 Mar 2024

In this application note, Thermo Fisher Scientific highlights a study that aims to demonstrate the applicability of the In-Tube Extraction Dynamic Headspace (ITEX-DHS) technique coupled to gas chromatography-mass spectrometry (GC-MS) for the determination of trace-level odorants in water. Through dynamic headspace enrichment achieved by means of the ITEX technique, the target analytes isoborneol (IB), 2-methyl-isoborneol (2-MIB), 2,4,6-trichloroanisole (2,4,6-TCA), and geosmin were extracted and pre-concentrated to reach sub-ppt level limits of detection (LOD).

Links

Tags

Gas ChromatographyGas chromatography (GC) is an analytical technique used to separate and quantitate mixtures of small and volatile compounds. Gas chromatographs or GC systems include components such as GC columns, detectors, pumps and autosamplers. Choose from packed or capillary GC columns, flame ionization (FID), photoionization (PID) electron capture detectors and selective or non-selective detectors. Find the best gas chromatographs in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Mass SpectrometryMass spectrometry (MS) is a powerful analytical technique used to identify and quantify molecules based on the mass-to-charge ratio of gas-phase ions. It provides detailed information about the structure, composition, and properties of compounds and is widely used across fields such as environmental monitoring, materials science, drug discovery and development, food and beverage testing, and wider chemical research. Key MS techniques include tandem mass spectrometry (MS/MS), liquid chromatography–mass spectrometry (LS-MS) and inductively coupled plasma (ICP-MS). Choosing from these wide range of techniques and technologies can be a daunting task, so keep up to date with scientific applications, performance expectations, and customer reviews here all in one place. Visit our product directory to receive quotes direct from the manufacturer. Sample ManagementSample management systems include sample storage devices such as freezers and plate storers, sample environment enclosures and sample organization, retrieval and sorter systems. Useful system features include high-throughput, automation, robotic arms, automated liquid handling and associated database systems. Accessories in sample management include barcode scanners, heat sealers and tubes.Environmental Monitoring and TestingEnvironmental monitoring and testing uses handheld portable analyzers, kits, spectrometers or chromatography systems for air, water, soil, food and other sample testing. Useful features of analyzers such as BOD and COD include portability, easy calibration, automation and sensitivity.  Environmental test kits for pH, water, moisture, etc, should be accurate, sensitive, reliable, fast and easy to use.Water PurificationThere are a number of water purification methods available to remove contamination from laboratory water. These systems include demineralization, reverse osmosis, filtration and ultrafiltration. A combination of methods is sometimes necessary to achieve purified water suitable for use in experiments.ChromatographyChromatography is a powerful technique used to separate and analyze components of mixtures based on their chemical properties. It is widely used in fields like biochemistry, pharmaceuticals, and environmental analysis. By exploiting differences in the interaction of substances with a stationary phase and a mobile phase, chromatography enables precise purification and quantification of compounds. Whether you're working with complex biological samples or industrial chemicals, chromatography is essential for obtaining high-quality results. Browse our peer-reviewed product directory to find the best chromatography systems, compare products, read customer reviews, and get pricing directly from manufacturers.Water AnalysisAnalytical methods used to test the purity of drinking water include determining the level of contaminants abides to the level set by the Environmental Protection Agency (EPA).Sample ConcentrationSample concentration involves the removal of solvents from samples using technologies such as centrifugal evaporation, lyophilization and rotary evaporation.Gas ChromatographyGas chromatography (GC) is an analytical technique used to separate and analyze gases or volatile liquids in a sample. It is widely used in environmental testing, food safety, pharmaceuticals, and forensic science. GC is ideal for identifying and quantifying compounds that are gaseous or can be vaporized without decomposition. Browse our peer-reviewed product directory to find the best gas chromatography systems, compare products, check reviews, and get pricing directly from manufacturers.
In-Tube Extraction Dynamic Headspace (ITEX-DHS) sampling technique coupled to GC-MS for sensitive determination of odorants in water