ResourceSpectroscopy

Diffraction Contrast Tomography: Unlocking Crystallographic Information from X-Ray Microscopy

6 Jun 2019

X-ray tomography has operated under two primary contrast mechanisms for some time: X-ray absorption and phase contrast, which both rely on material density differences within the sample. However, single-phase polycrystalline materials (e.g. steels, alloys, etc.) do not exhibit any significant contrast using absorption or phase mechanisms. Synchrotron-based XRM has demonstrated results in this area for about a decade with diffraction contrast tomography (DCT), which provides crystallographic/diffraction information from polycrystalline samples, non- destructively, in 3D. Now, advancing laboratory X-ray microscopy (XRM) one step further, ZEISS describes the capabilities of laboratory- based DCT on the ZEISS Xradia 620 Versa 3D X-ray microscope, and the new research and characterization capabilities this enables.

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X-ray CrystallographyX-ray crystallography is an analytical technique used to determine the arrangement of atoms in a crystal. Monochromatic x-rays are produced from a synchrotron or x-ray generator. An x-ray crystallography system uses a detector to measure the x-ray diffraction from the crystal. The information is used to generate a 3D image of the crystal.X-Ray Diffraction and SpectroscopyX-Ray diffraction & spectroscopy are used in material characterization to discern the structure and elemental composition of a sample. X-Ray diffractometers (XRD) are superior instruments in elucidating the dimensional atomic structure of crystalline materials, including powders, thin films and single crystals. For large unit cells or ordered macromolecules, consider small-angle X-ray scattering (SAXS). X-ray spectroscopic techniques include X-ray fluorescence (XRF) and X-ray photoelectron spectroscopy (XPS), both providing simple and accurate methods for determining the elemental composition of a material. Energy dispersive (EDXRF) and wavelength dispersive (WDXRF) XRF spectrometers are available, as well as handheld/portable devices. High-resolution, 3D microstructure characterization of materials can be achieved with X-ray microscopes combining sub-micron resolution imaging with 3D computed tomography. Find the best XRD and XRF spectrometers in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.MicroscopyMicroscopy is a technique used to observe small objects in detail, from cells to materials, using light or electron microscopes. It enables researchers to examine structures with high resolution, aiding in fields such as biology, medicine, and materials science. With advanced microscopy techniques, scientists can gain insights into cellular processes, tissue structures, and material properties. Explore the best microscopy solutions in our peer-reviewed product directory, compare products, read customer reviews, and get pricing directly from manufacturers.Crystallography
Diffraction Contrast Tomography: Unlocking Crystallographic Information from X-Ray Microscopy