ResourceSpectroscopy

Diffraction Contrast Tomography: Unlocking Crystallographic Information from Laboratory X-ray Microscopy

10 May 2017

X-ray tomography has operated under two primary contrast mechanisms for some time: X-ray absorption contrast, providing density information, and phase propagation contrast, providing enhanced interfacial information. These primary mechanisms are powerful and advanced laboratory-scale X-ray microscopy (XRM) platforms have demonstrated great improvements to this in recent years. XRM is enabling an additional modality known as diffraction contrast tomography (DCT) that provides crystallographic/diffraction information from polycrystalline samples, facilitating the ability to directly characterize a samples crystalline microstructure, non-destructively. This application note describes the capabilities of lab DCT on the ZEISS Xradia 520 Versa platform, and new research and characterization capabilities it enables.

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X-ray CrystallographyX-ray crystallography is an analytical technique used to determine the arrangement of atoms in a crystal. Monochromatic x-rays are produced from a synchrotron or x-ray generator. An x-ray crystallography system uses a detector to measure the x-ray diffraction from the crystal. The information is used to generate a 3D image of the crystal.X-Ray Diffraction and SpectroscopyX-Ray diffraction & spectroscopy are used in material characterization to discern the structure and elemental composition of a sample. X-Ray diffractometers (XRD) are superior instruments in elucidating the dimensional atomic structure of crystalline materials, including powders, thin films and single crystals. For large unit cells or ordered macromolecules, consider small-angle X-ray scattering (SAXS). X-ray spectroscopic techniques include X-ray fluorescence (XRF) and X-ray photoelectron spectroscopy (XPS), both providing simple and accurate methods for determining the elemental composition of a material. Energy dispersive (EDXRF) and wavelength dispersive (WDXRF) XRF spectrometers are available, as well as handheld/portable devices. High-resolution, 3D microstructure characterization of materials can be achieved with X-ray microscopes combining sub-micron resolution imaging with 3D computed tomography. Find the best XRD and XRF spectrometers in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.CrystallographyX-ray MicroscopyX-Ray Tomography
Diffraction Contrast Tomography: Unlocking Crystallographic Information from Laboratory X-ray Microscopy