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Determination of Pesticide Residues in Marijuana by QuEChERS and LC-MS/MS

UCT, Inc.
30 Jan 2015

The medical use of marijuana has been legalized in many states in the USA. With this limited legalization and use of marijuana, the determination of pesticide residues becomes important. Patients taking medical marijuana in conjunction with other therapies may be more vulnerable to toxic substances, such as pesticides. This poster presents a robust and efficient method using the AOAC QuEChERS and LC-MS/MS techniques to determine pesticide concentrations in marijuana samples.

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ChloroFiltr® for QuEChERS dSPE Clean-Up

UCT, Inc.

Chlorophyll in QuEChERS extracts must be removed to reduce potential instrument downtime. This is removed from extracts using graphitized carbon black (GCB) Unfortunately, GCB also removes planar analytes reducing analytical accuracy. ChloroFiltr®, used in place of GCB in dSPE tubes, removes unwanted chlorophyll without removing pesticides or environmental analytes. No change in procedure are required.

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QuEChERS

UCT, Inc.

QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe) is a sample extraction and clean-up technique used for the analysis of multiple pesticide residues in agricultural products. UCT manufactures a wide variety of pre-filled tubes and reagent pouches for all QuEChERS method variations including PSA, C18, buffers, anh. MgSO4, NaCl, ChloroFiltr, and carbon.

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LC-MSLC-MS (liquid chromatography-mass spectrometry) systems and equipment are used for separation and quantitative analysis of complex mixtures, combining liquid chromatography and mass spectrometry. Quantify proteins, contaminants, pesticides or screen for drug metabolites with a high level of sensitivity. LC-MS systems and equipment include reverse phase, normal phase and specialized columns integrated with various MS detectors such as time-of-flight (TOF), quadrupole, orbitrap or ion trap mass analyzers. LC-MS/MS instruments equipped with a qTOF or triple quadrupole analyzer give greater sensitivity and resolving power to your analysis. Find the best LC-MS equipment in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.QuEChERSThe QuEChERS (Quick, Easy, Cheap, Effective, Rugged, and Safe) method is a streamlined approach that is used to extract multi-residue target compounds from food samples. It is most commonly used by analytical chemists studying pesticide residues in food.PesticidesPesticides are used to protect crops from diseases, pests and unwanted plants. They are classed as persistent organic pollutants (POPs) and can be harmful to humans. The Environmental Protection Agency (EPA) currently regulates the use of pesticides in the USA.

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Determination of Pesticide Residues in Marijuana by QuEChERS and LC-MS/MS