Determination of Highly Polar Pesticide Residues in Food of Plant Origin by an Automated QuPPe Solution

22 Jan 2016

This application note evaluates the performance and versatility of the AutoMate-Q40 for the extraction of highly polar pesticides using the QuPPe Method. Liquid Chromatography coupled to triple-quadrupole mass spectrometry (LC-MS/MS) was employed for the detection of highly polar pesticides in agricultural commodities. Quantification was based on matrix-matched calibration curves for each commodity. The AutoMate-Q40 streamlines the QuPPe Method while providing suitable analytical results falling in the method guidelines (range of 70-120% and RSD <20%) for all target compounds.

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LC-MSLC-MS (liquid chromatography-mass spectrometry) systems and equipment are used for separation and quantitative analysis of complex mixtures, combining liquid chromatography and mass spectrometry. Quantify proteins, contaminants, pesticides or screen for drug metabolites with a high level of sensitivity. LC-MS systems and equipment include reverse phase, normal phase and specialized columns integrated with various MS detectors such as time-of-flight (TOF), quadrupole, orbitrap or ion trap mass analyzers. LC-MS/MS instruments equipped with a qTOF or triple quadrupole analyzer give greater sensitivity and resolving power to your analysis. Find the best LC-MS equipment in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Automated Liquid HandlingAutomated liquid handling equipment is used to mix, dilute and dispense allotted volumes of liquid into microplates and other vessels automatically. The robotic, liquid handling arms can dispense from single channel to 3456 multichannel as well as operate nanoliter dispensing, enabling high throughput of samples. Find the best automated liquid handlers in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.PesticidesPesticides are used to protect crops from diseases, pests and unwanted plants. They are classed as persistent organic pollutants (POPs) and can be harmful to humans. The Environmental Protection Agency (EPA) currently regulates the use of pesticides in the USA.