ResourceGeneral Lab

Concentrating extract in a rotavap

10 Mar 2020

After winterized extract has been filtered, a rotary evaporator, or rotavap, is used to concentrate the extract by evaporating off most of the remaining ethanol. Major objectives in this process are to quickly concentrate the mixture of crude oil and ethanol to the point where it is only a few percent ethanol, to recover the evaporated ethanol for later use, and to keep the evaporation process under control to prevent loss of crude oil. In this application note, BrandTech demonstrates solutions for better rotary evaporation, designed to help accelerate production and maximize solvent recovery.

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PumpsLaboratory pumps are devices used to move liquids and gases by vacuum or positive displacement. The pressures/vacuums generated are determined by the type of pump used. High vacuum pumps include diffusion, ion, roots and turbopumps; for primary/medium vacuum applications see rotary vane pumps, scroll & diaphragm pumps. For the positive displacement of liquids explore a range of syringe and peristaltic pumps, as well as fluid aspirators. Discover the best pumps in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Evaporators and Freeze DryersCentrifugal evaporation is used for solvent removal from a sample. This is a useful technique for sample concentration or sample drying. Many centrifugal evaporators are modular with a central vacuum pump for generating low pressure. Useful features of evaporators or vacuum ovens include minimal solvent bumping, solvent resistance, computer control, temperature regulation and benchtop design.Crude OilThe chemical evaluation of the complex combination of hydrocarbons and organometallic compounds found within crude oil. The results provide data on the chemical characteristics of a sample for petroleum testing laboratories.EthanolSolvent ExtractionSolvent Evaporation
Concentrating extract in a rotavap