Quantachrome Instruments Releases the XeriPrep™ Sample Preparation Degasser

1 Aug 2013
Sarah Thomas
Associate Editor

Product news

This degasser is used to dry (Xeri is derived from the Greek word “xeros” meaning “dry”), samples prior to surface area and pore size analysis by gas sorption. The XeriPrep™ can be used with a variety of Quantachrome’s gas sorption analyzers including the Autosorb® 6 iSA™, Autosorb® iQ, Nova™ Series, Quadrasorb™, and iSorb™.

Consistent and reliable surface area and pore size analysis depend upon proper sample preparation. This “degassing” involves the removal of surface moisture and other contaminants by heating the sample under vacuum. The XeriPrep™ provides the necessary accurate and consistent sample preparation required by high-throughput
physisorption analyzers.

The XeriPrep™ degasser has six preparation stations side-by-side for easy access; each station having its own heater for independent operation – up to 350°C (662°F) is standard, optionally up to 450°C (842°F).

The XeriPrep™ provides PC control of all six heaters with individual protocols consistent of programmable heating ramp and times. All six stations accept three sizes of sample cell diameters using fittings that can be adapted quickly and easily without tools. The built in cold trap provides for efficient removal of condensables at low degassing temperatures and for a clean and efficient vacuum at all degassing temperatures. The standard version of the XeriPrep™ includes a two-stage vacuum pump with the option of adding a turbo pump for rapid high vacuum degassing. Also included is a digital vacuum gauge for establishing completeness of sample readiness after degassing.

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UHPLC and HPLCHigh performance liquid chromatography (HPLC) and ultra high performance liquid chromatography (UHPLC), also known as UPLC, are analytical techniques used to separate, identify and quantitate components of complex mixtures including biological samples such as proteins and lipids as well as chemical mixtures of pesticides, drugs and oils. Both techniques are liquid chromatographic methods but differ by operating pressures (HPLC < 6000 psi < UHPLC ). Components of HPLC and UHPLC systems include columns, detectors, pumps, autosamplers and column heaters. Explore a range of UHPLC and HPLC columns for your specific sample needs including reverse phase, normal phase, ion exchange, HILIC, ion exclusion and size exclusion columns. For more specialized HPLC, explore FPLC, countercurrent LC and simulated moving bed systems. Find the best UHPLC and HPLC equipment in our peer reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Sample PreparationSample preparation can improve the quality and speed of separation techniques. Products to assist sample preparation include filtration equipment, evaporators, membranes and sieves.Particle CharacterizationParticle characterization instruments are used to determine particle size distribution, shape, surface area, zeta potential, density and porosity of particles and materials. Multiple tecchniques are available for determining particle size, shape and count including dynamic light scattering (DLS), laser diffraction, electrozone (Coulter technique), imaging particle analysis and single particle optical sensing. Determine the density of your material with a gas pycnometer or examine its surface area and porosity with gas adsorption analyzers and mercury porosimeters. Find the best particle characterization instruments in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Sample HandlingProper and careful handling of samples is important in scientific studies to ensure the integrity of specimens. This will prevent deterioration and cross contamination, and improve the accuracy of sample tracking procedures.
Quantachrome Instruments Releases the XeriPrep™ Sample Preparation Degasser