New High Temperature GPC/SEC System with Improved Sensitivity and Automation for Polyolefin Analysis

9 Aug 2012
Tesni Perry
Administrator / Office Personnel

Product news

Polymer Char announces the development of a renewed reliable and fully automated 4D Gel Permeation Chromatography (GPC/SEC) system with a significant improvement in the IR detectors to measure the composition and molar mass of polyolefins.

The new GPC-IR instrument incorporates new features such as the full integration of the new infrared detector IR5 MCT, with outstanding sensitivity and stability to measure both concentration and composition (SCB/1000C). In addition, other detectors such as a four capillary bridge viscometer and a multi-angle light scattering for Long Chain Branching (LCB) can be coupled to Polymer Char GPC-IR becoming the most advanced instrumentation for SEC analyses.

The GPC-IR automates all sample preparation steps, including the initial vials filling as well as an in-line filtration with blackflush cleaning. As a result, neither vials transfer nor manual solvents handling is required at any moment throughout the whole analytical process.

Polymer Char's GPC-IR incorporates other technological developments, based on the principles of most reliable hardware, full automation, user friendly operation, easy maintenance and proper diagnostic tools. Some of these features developed are for instance the ones related to the sample care to minimize degradation, that is, taking only the necessary time to complete dissolution for each vial (no longer than desired), shaking instead of stirring and N2 vials purge. Furthermore, other important advantages are introduced like a column compartment, independent from the rest of the hardware, a solvent recycling system or a very comprehensive calculations software (GPC One) developed with the industry leaders, integrating all detectors signals.

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Size Exclusion ChromatographySize exclusion chromatography (SEC) is a liquid chromatographic technique used to separate and identify molecules based on their size, including polymers, proteins, nanoparticles & nucleic acid. SEC is further subdivided into gel filtration chromatography (GFC) and gel permeation chromatography (GPC) when an aqueous or organic mobile phase is used respectively. HPLC-based SEC systems and columns are available for analytical separation alongside SEC spin columns or filters to prep samples for many protocols. Find the best size exclusion chromatography equipment in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Infrared / IR SpectroscopyInfrared (IR) spectroscopy measures the interaction of infrared light with a sample, including transmission, reflectance & absorbance, facilitating the identification of analytes. Equipment used for quantitative analysis includes Fourier-transform infrared (FTIR) spectrometers, infrared cameras, FTIR gas analyzers, as well as attenuated total reflectance (ATR) accessories and pellet or film presses. Find the best IR spectroscopy products in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.PolymersPolymers are large molecules made up of many repeat units. Natural polymers such as DNA and proteins are essential to life, whereas synthetic polymers such as polystyrene and polyethylene are used widely due to their functionality. Typical techniques for analysis include GPC, SEC, DSC, FT-IR and NMR.Polyolefins
New High Temperature GPC/SEC System with Improved Sensitivity and Automation for Polyolefin Analysis