Meeting the Growing Challenges of Pesticides and Contaminants – Special Feature

From field to food discover the technology scientists are using to monitor food and environmental samples in this special feature

3 Apr 2018
Emily Adam
Publishing / Media

Editorial article

In April SelectScience® is focusing on the impact that pesticides and other contaminants have on our environment and food, and how this is driving the development of new sensitive and accurate technologies. In this feature you can discover methods for detecting these contaminants in a range of matrices and useful resources from across the industry to help your lab workflow.

THE WORLD'S GROWING APPETITE: How Will We Ensure Safe, Nutritional Food Production in Years to Come?

From insecticide contamination in eggs to salmonella scares in baby formula, concerns around food safety rarely leave the news. The safety of our food can be compromised both inadvertently through pesticide contamination and through purposeful adulteration. As the global food market is put under pressure, managing the safety of our food will remain a top priority. Discover the solutions scientists predict will be utilized in the future to overcome these challenges. Visit Feature

 

FOOD SUPPLY QUALITY: Comprehensive Pesticide Residue Analysis by LC/MS/MS

With recent contamination issues in a wide range of commodities, ensuring the quality of our food supply is becoming increasingly important. Pesticide residue content is one area of concern. LC/MS/MS can be used to simultaneously monitor hundreds of potential contaminants, including those difficult to detect by GC. Using LC/MS/MS in combination with GC allows for a faster, more complete picture of pesticide residues.

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ENHANCED REPORTING CONFIDENCE: Routine Pesticide Residue Analysis


Discover how you can help reduce the incidence of false positive and negative reporting in pesticide residue monitoring. This application note describes enhanced routine multiple-reaction monitoring (MRM) methods to detect a higher number of fragment ion transitions for increased specificity and reporting confidence. In this workflow, typically 6-10 fragment ion transitions were monitored for each target pesticide as opposed to a conventional approach using 2-3 fragment ions only.

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UNDERSTANDING EPA 538: Determining Organic Contaminants in Drinking Water

Discover the method for preparation and analysis of drinking water samples to detect and measure acephate, diisopropyl methylphosphonate (DIMP), methamidophos and thiofanox. In this application note find out how the Selectra® Aqueous C18 HPLC Column from UCT can be used to accurately detect selected organic contaminants in drinking water by aqueous direct injection and LC/MS/MS.

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TOXICITY TESTING: Custom-Made Multiplex Assays Aid Unique Agrochemical Analysis


Hormone-altering chemicals can cause developmental problems during pregnancy, abnormal growth patterns, abnormal reproductive function and also trigger some forms of cancer when ingested. In this SelectScience® interview, Dr. Olivier Blanck, from the Crop Science division of Bayer in France, explores the importance of examining toxicity during agrochemical development and discusses current projects under the endocrine disruption program.

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OPTIMIZED WATER ANALYSIS: How to Ensure Quality Control & Meet Regulatory Requirements

In this video, Dr Edward F. Askew tackles some of the frequently asked questions about the water analysis industry regulations and quality control, as well as pinpointing the benefits of Spectroquant Test Kits for this application. Dr Askew is President of Askew Scientific Consulting LLC, a research lab and consultancy that has worked with Merck KGaA to produce the kits which are designed to meet method equivalency for EPA, clean water act methods and safe drinking water act methods.

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SELECTRA® HPLC Columns

UCT, Inc.

High purity, Type B, spherical silica support. 100A pore size. 1.8um, 3um, & 5um partical sizes. Variety of stationary phases.

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Ultra Aqueous C18 Columns

Restek Corp.

The Ultra line represents Restek’s broadest selection of stationary phases on a single silica support. Made of high-purity, type-B silica that minimizes activity and creates high-density bonding, these columns are designed for selective and reliable HPLC applications.The Ultra Aqueous C18 HPLC column provides reproducible retention times and can be used with highly aqueous mobile phases, which may eliminate the need for sample derivitization or ion pairing reagents. This column features a true C18 alkyl bonded phase, meeting the requirements of a US Pharmacopoeia (USP) L1 stationary phase.The Ultra Aqueous C18 column uses a novel bonding chemistry that results in polar groups at the silica surface. These surface polar groups keep the alkyl stationary phase extended, and thus wetted by the mobile phase—even when using up to 100% aqueous mobile phases.Additionally, although the Ultra Aqueous C18 column behaves similarly to a traditional base-deactivated C18 column when analyzing neutral hydrophobic compounds, it has enhanced retention and unique selectivity for polar and basic compounds.Ultra Aqueous C18 Columns Features: Analyzes polar compounds by reversed phase. Retains compounds such as amino acids and water soluble vitamins using simple mobile phases and without derivitization. Analyzes polar, hydrophillic materials without retention time loss. Stable retention in 100% aqueous mobile phases. Can analyze compounds that are sparingly soluble in organic solvents. True C18 alkyl bonded phase. High-density C18 ligand coverage. Similar selectivity as traditional C18 phases for neutral hydrophobic compounds. Unique secondary polar characteristics. End-capping diminishes peak tailing observed from exposed silanol sites on the silica surface. Column Characteristics: Phase: C18 particle Size: 3, 5 μm Pore Size: 100 Å Length: 30, 50, 100, 150, 200, 250 mm ID: 0.3, 1.0, 2.1, 3.0, 3.2, 4.6 mm

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UHPLC and HPLCHigh performance liquid chromatography (HPLC) and ultra high performance liquid chromatography (UHPLC), also known as UPLC, are analytical techniques used to separate, identify and quantitate components of complex mixtures including biological samples such as proteins and lipids as well as chemical mixtures of pesticides, drugs and oils. Both techniques are liquid chromatographic methods but differ by operating pressures (HPLC < 6000 psi < UHPLC ). Components of HPLC and UHPLC systems include columns, detectors, pumps, autosamplers and column heaters. Explore a range of UHPLC and HPLC columns for your specific sample needs including reverse phase, normal phase, ion exchange, HILIC, ion exclusion and size exclusion columns. For more specialized HPLC, explore FPLC, countercurrent LC and simulated moving bed systems. Find the best UHPLC and HPLC equipment in our peer reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Atomic Absorption / Emission SpectroscopyAtomic absorption spectroscopy (AAS) and atomic emission spectroscopy (AES) — also called optical emission spectroscopy (OES) — are used to detect the elemental constituents in samples. Both techniques involve the atomization of a sample. Atomic absorption spectrometers may use a flame or furnace to create an atomic vapor of the sample before irradiation with spectral light. Optical emission spectrometers may use a flame, inductively coupled plasma (ICP), microwave plasma (MP) or spark arcs to atomize and excite the sample. At higher excitation energies, electrons can be emitted instead of photons, which can be useful for samples that can’t be atomized and for surface analysis. Explore electron spectroscopy equipment such as Auger spectrometers and photoelectron spectrometers for surface elemental analysis of samples. Find the best atomic absorption, photoelectron and optical emission spectrometers in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Environmental Monitoring and TestingEnvironmental monitoring and testing uses handheld portable analyzers, kits, spectrometers or chromatography systems for air, water, soil, food and other sample testing. Useful features of analyzers such as BOD and COD include portability, easy calibration, automation and sensitivity.  Environmental test kits for pH, water, moisture, etc, should be accurate, sensitive, reliable, fast and easy to use.Particle CharacterizationParticle characterization instruments are used to determine particle size distribution, shape, surface area, zeta potential, density and porosity of particles and materials. Multiple tecchniques are available for determining particle size, shape and count including dynamic light scattering (DLS), laser diffraction, electrozone (Coulter technique), imaging particle analysis and single particle optical sensing. Determine the density of your material with a gas pycnometer or examine its surface area and porosity with gas adsorption analyzers and mercury porosimeters. Find the best particle characterization instruments in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.GC-MS GC-MS (gas chromatography-mass spectrometry) instruments and equipment are used to separate, quantify and identify mixtures of small and volatile compounds, such as polycyclic aromatics, fatty acids and alcohols. Often used in drug detection, forensic investigation and environmental analysis for pesticides and contaminants, GC-MS is a powerful addition to your lab’s analytical capabilities. GC-MS/MS instruments equipped with a qTOF or triple quadrupole analyzers can give greater sensitivity and resolution to your analysis. Find the best GC-MS instruments and equipment in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Water PurificationThere are a number of water purification methods available to remove contamination from laboratory water. These systems include demineralization, reverse osmosis, filtration and ultrafiltration. A combination of methods is sometimes necessary to achieve purified water suitable for use in experiments.PesticidesPesticides are used to protect crops from diseases, pests and unwanted plants. They are classed as persistent organic pollutants (POPs) and can be harmful to humans. The Environmental Protection Agency (EPA) currently regulates the use of pesticides in the USA. Water AnalysisAnalytical methods used to test the purity of drinking water include determining the level of contaminants abides to the level set by the Environmental Protection Agency (EPA).Food ContaminationFood contamination refers to the presence of harmful substances or pathogens in food, posing risks to human health. Contaminants can be biological, chemical, or physical, and their detection is crucial for ensuring food safety. Advanced testing methods like PCR, chromatography, and spectroscopy are used to identify contaminants in food products. Browse our peer-reviewed product directory to find the best solutions for food contamination detection, compare products, check reviews, and get pricing directly from manufacturers.Environmental ContaminationContaminants in the environment are harmful chemicals that are present in the air, land and water. These include pesticides, pharmaceuticals, persistent organic pollutants (POPs) and many more.