Freeman Technology and Particle Technology Labs’ collaboration takes powder characterization service to new levels

24 Oct 2007
Greg Smith
Analyst / Analytical Chemist

Product news

A specialist team of analysts has been introduced to manage the growing workload generated by increased uptake of the powder characterization service offered by Particle Technology Labs Ltd (PTL) (Chicago, US). The service, which is built around the use of the Freeman Technology FT4 Powder Rheometer, was introduced at Pittcon in 2005.

It has been fully operational for more than two years and demand has increased significantly this year. Since the inception of the service a wide range of industrial powders has been tested, including ceramics, cement and pharmaceutical materials.

PTL is an established laboratory that is highly experienced in the characterization of fine particles. The powder characterization service was established in response to a growing demand from clients who wanted more information about the flow properties of their powders.

Bill Kopesky, Laboratory Manager at PTL confirmed the benefits that their clients are seeing. “Using the FT4 we undertake a series of flowability studies with the dynamic testing regimes available on the instrument. We also use it for shear testing where required. If two powders behave differently, or a powder’s behaviour changes, then we can really start to examine the differences,” he said. “Clients have, for example, been able to use the data we generate to allow them to change a formulation, and clearly monitor the results. People tend to be very impressed at the degree of sensitivity that can be achieved in showing differences between powders.”

The lab also acts as a reference site in North America for the FT4 and operates the powder characterization service in close conjunction with Freeman Technology. The powder processing experience and expertise of the Freeman team provides additional support on data interpretation and in relating results back to real-world processing situations.

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RheometryRheometers are used to measure the rheology of fluids, which is the flow of fluids in response to an applied force. The most common types of rheometer include shear rheometers (capillary, cone and plate and rotational cylinder) and extensional rheometers. Viscometers are similar to rheometers however viscometers only measure the viscosity of a fluid.Particle CharacterizationParticle characterization instruments are used to determine particle size distribution, shape, surface area, zeta potential, density and porosity of particles and materials. Multiple tecchniques are available for determining particle size, shape and count including dynamic light scattering (DLS), laser diffraction, electrozone (Coulter technique), imaging particle analysis and single particle optical sensing. Determine the density of your material with a gas pycnometer or examine its surface area and porosity with gas adsorption analyzers and mercury porosimeters. Find the best particle characterization instruments in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.
Freeman Technology and Particle Technology Labs’ collaboration takes powder characterization service to new levels