Fighting Food Fraud – Is My Olive Oil Authentic

Improving detection of food adulteration with the latest MS technology

22 Dec 2016
Sarah Thomas
Associate Editor

Editorial article

Dr Khalil Divan, Senior Director Global Marketing: Food & Beverage, Thermo Fisher Scientific

Dr Khalil Divan, senior director of global marketing group, food & beverage, within Thermo Fisher Scientific discusses how cutting edge mass spectrometry technology is being used to help fight food fraud. SelectScience® Editor, Dr Lois Manton-O’Byrne, spoke with Dr Divan at the 53rd Annual North American Chemical Residue Workshop (NACRW), about the latest methods and technologies being employed.

LMOB: What is food fraud and what are the implications for the food and beverage industry?

KD: Food fraud is a term used where food products are either mislabelled or adulterated for economic gains. Food authenticity is very important. If you buy extra virgin olive oil from Italy, the consumer expects that the product is extra virgin olive oil from Italy. Food adulteration is a big concern in this area, where people add alternative ingredients to the product which are cheaper than the actual ingredients that make up the component in the food product.

Fraud costs the food and beverage industry billions of dollars a year so it’s very important to ensure that the product and the raw ingredients used are not adulterated, or are authentic from the perspective of what the consumer is receiving.

LMOB: What is the biggest challenge in food fraud testing?

KD: The big challenge in authenticity testing or food adulteration, is that nobody tells you what they’ve adulterated it with or where the product has actually come from.

LMOB: What key technologies are used to detect food fraud?

KD: Isotope ratio mass spectrometry is used to identify isotopic differences in various products. You can actually detect a pattern that identifies where the product has come from just by looking at the isotopic ratio. In the area of honey testing or olive oil testing, isotope-ratio technology that we offer has been used extensively.

You also need screening technologies. The introduction of Orbitrap technology both on the gas and liquid chromatography platform, offers the ideal technology for customers who are looking for unknown screening so they can screen a sample and identify compounds which could potentially have been added to the product.

LMOB: What do you hear from your customers?

KD: Our customers want solutions. What we mean by solutions is they’re looking to us to partner with them to supply the, conditions for sample preparation, the method, right up to the instrument conditions. Our aim is to provide a total workflow so all the customer has to do is put in the matrix that they’re interested in, the analytes that they want to monitor, download the method onto the instrument and then the instrument is ready to run from day one. Saving our customers the time and effort in developing workflows from scratch. By providing workflows from sample preparation to data they can quickly turn it into knowledge so they can use it to focus on the science and business needs.

LMOB: What do you hear from the food and beverage industry regulators?

KD: What the industry and the regulators are looking for from our perspective is to provide technology and innovations which address two key areas - more sensitive instrumentation, to comply with the lowering of detection limits for key analytes in the area of food safety, and also innovations which address a wide range of analytes in one run - Multi residue methods. By developing solutions we also will be helping our customers to be more efficient and increase their productivity by reducing training needs, method development time and comply with regulations covering food safety, monitor quality of their product, meet labelling requirements and combat food fraud.

Watch the video interview or visit the NACRW special feature to learn more.

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LC-MSLC-MS (liquid chromatography-mass spectrometry) systems and equipment are used for separation and quantitative analysis of complex mixtures, combining liquid chromatography and mass spectrometry. Quantify proteins, contaminants, pesticides or screen for drug metabolites with a high level of sensitivity. LC-MS systems and equipment include reverse phase, normal phase and specialized columns integrated with various MS detectors such as time-of-flight (TOF), quadrupole, orbitrap or ion trap mass analyzers. LC-MS/MS instruments equipped with a qTOF or triple quadrupole analyzer give greater sensitivity and resolving power to your analysis. Find the best LC-MS equipment in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Mass SpectrometryMass spectrometry (MS) is a powerful analytical technique used to identify and quantify molecules based on the mass-to-charge ratio of gas-phase ions. It provides detailed information about the structure, composition, and properties of compounds and is widely used across fields such as environmental monitoring, materials science, drug discovery and development, food and beverage testing, and wider chemical research. Key MS techniques include tandem mass spectrometry (MS/MS), liquid chromatography–mass spectrometry (LS-MS) and inductively coupled plasma (ICP-MS). Choosing from these wide range of techniques and technologies can be a daunting task, so keep up to date with scientific applications, performance expectations, and customer reviews here all in one place. Visit our product directory to receive quotes direct from the manufacturer. GC-MS GC-MS (gas chromatography-mass spectrometry) instruments and equipment are used to separate, quantify and identify mixtures of small and volatile compounds, such as polycyclic aromatics, fatty acids and alcohols. Often used in drug detection, forensic investigation and environmental analysis for pesticides and contaminants, GC-MS is a powerful addition to your lab’s analytical capabilities. GC-MS/MS instruments equipped with a qTOF or triple quadrupole analyzers can give greater sensitivity and resolution to your analysis. Find the best GC-MS instruments and equipment in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Food SafetyFood safety describes the prevention of food-borne illnesses. Contamination with a variety of pathogens can be prevented with adequate temperature control, hygiene and labeling. Food samples can be tested using GC/MS, HPLC, SPE, and qPCR to ensure their adherence to regulations.Food AuthenticationFood authentication ensures that food products are accurately labeled and free from adulteration or misrepresentation. This is important for consumer safety, quality control, and regulatory compliance. Explore food authentication tools in our peer-reviewed product directory; compare products, check reviews, and get pricing directly from manufacturers.AdulterationFood QualityFood quality refers to the attributes of food that influence its safety, nutrition, and taste. Monitoring and ensuring food quality are essential in production to meet health regulations and consumer expectations. Techniques like spectroscopy, chromatography, and microbial testing are used to assess food properties and detect contaminants. Browse our peer-reviewed product directory to find food quality testing solutions; compare products, check reviews, and get pricing directly from manufacturers.Food FraudFood adulteration refers to food when it has been has been altered unlawfully with the addition of another lower commodity food product to increase quantity. The 2013 European horsemeat scandal saw the adulteration of beef products with the addition of horse meat.